TY - JOUR
T1 - Determination of isoflavone glucoside malonates in Trifolium pratense L. (red clover) extracts: quantification and stability studies
AU - Drs. de Rijke, E.
AU - Zafra-Gomez, A.
AU - Ariese, F.
AU - Brinkman, U.A.T.
AU - Gooije, C.
PY - 2001
Y1 - 2001
N2 - Isoflavones, their glucosides and their glucoside malonates were determined in red clover leaf extracts using reversed-phase LC coupled to atmospheric pressure chemical ionisation mass spectrometry (APCI-MS), UV and fluorescence detectors and the stability of the malonates was investigated. Extracts can be stored at least 1-2 weeks at -20°C without loss of malonates. In LC-separated fractions the malonates are most stable when stored at low temperature after evaporation to dryness. The concentrations of eight major isoflavones ranged from 0.04 to 5 mg/g leaves. © 2001 Elsevier Science B.V. All rights reserved.
AB - Isoflavones, their glucosides and their glucoside malonates were determined in red clover leaf extracts using reversed-phase LC coupled to atmospheric pressure chemical ionisation mass spectrometry (APCI-MS), UV and fluorescence detectors and the stability of the malonates was investigated. Extracts can be stored at least 1-2 weeks at -20°C without loss of malonates. In LC-separated fractions the malonates are most stable when stored at low temperature after evaporation to dryness. The concentrations of eight major isoflavones ranged from 0.04 to 5 mg/g leaves. © 2001 Elsevier Science B.V. All rights reserved.
UR - https://www.scopus.com/pages/publications/0035850737
UR - https://www.scopus.com/inward/citedby.url?scp=0035850737&partnerID=8YFLogxK
U2 - 10.1016/S0021-9673(01)01231-6
DO - 10.1016/S0021-9673(01)01231-6
M3 - Article
SN - 0021-9673
VL - 932
SP - 55
EP - 64
JO - Journal of Chromatography A
JF - Journal of Chromatography A
IS - 1-2
ER -
