Effect of cement layer thickness on the immediate and long-term bond strength and residual stress between lithium disilicate glass-ceramic and human dentin

João Paulo Mendes Tribst*, Alison Flavio Campos Dos Santos, Giuliane da Cruz Santos, Larissa Sandy da Silva Leite, Julio Chávez Lozada, Laís Regiane Silva-Concílio, Kusai Baroudi, Marina Amaral

*Corresponding author for this work

Research output: Contribution to JournalArticleAcademicpeer-review

Abstract

This study tested whether three different cement layer thicknesses (60, 120 and 180 µm) would provide the same bonding capacity between adhesively luted lithium disilicate and human dentin. Ceramic blocks were cut to 20 blocks with a low-speed diamond saw under cooling water and were then cemented to human flat dentin with an adhesive protocol. The assembly was sectioned into 1 mm2 cross-section beams composed of ceramic/cement/dentin. Cement layer thickness was measured, and three groups were formed. Half of the samples were immediately tested to evaluate the short-term bond strength and the other half were submitted to an aging simulation. The microtensile test was performed in a universal testing machine, and the bond strength (MPa) was calculated. The fractured specimens were examined under stereomicroscopy. Applying the finite element method, the residual stress of polymerization shrinkage according to cement layer thickness was also calculated using first principal stress as analysis criteria. Kruskal–Wallis tests showed that the “cement layer thickness” factor significantly influenced the bond strength results for the aged samples (p = 0.028); however, no statistically significant difference was found between the immediately tested groups (p = 0.569). The higher the cement layer thickness, the higher the residual stress generated at the adhesive interface due to cement polymerization shrinkage. In conclusion, the cement layer thickness does not affect the immediate bond strength in lithium disilicate restorations; however, thinner cement layers are most stable in the short term, showing constant bond strength and lower residual stress.

Original languageEnglish
Article number5153
JournalMaterials
Volume14
Issue number18
DOIs
Publication statusPublished - Sept 2021

Bibliographical note

Funding Information:
This research was funded by Funda??o de Amparo ? Pesquisa do Estado de S?o Paulo grant number FAPESP 2019/20801-4 and Universidade de Taubat? with studentship PRPPG ODO_296_2019.

Publisher Copyright:
© 2021 by the authors. Licensee MDPI, Basel, Switzerland.

Funding

This research was funded by Funda??o de Amparo ? Pesquisa do Estado de S?o Paulo grant number FAPESP 2019/20801-4 and Universidade de Taubat? with studentship PRPPG ODO_296_2019.

FundersFunder number
Universidade de TaubatéODO_296_2019
Fundação de Amparo à Pesquisa do Estado de São Paulo2019/20801-4

    Keywords

    • Dental bonding
    • Dental materials
    • Finite element analysis
    • Polymerization

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