Effect of different finishing/polishing techniques and glaze application on the flexural strength of ultratranslucent zirconia after hydrothermal aging

Sarah Emille Gomes da Silva, Bianca Cristina Dantas da Silva, Anne Heloyse Teixeira Crispim, Amanda Maria de Oliveira Dal Piva, Cornelis Johannes Kleverlaan, Rodrigo Othávio de Assunção e. Souza*

*Corresponding author for this work

Research output: Contribution to JournalArticleAcademicpeer-review

Abstract

Purpose: To evaluate the effect of different finishing/polishing procedures and glaze on the surface roughness, flexure strength, and microstructure of an ultratranslucent zirconia (UZ) submitted aging. Methodology: Two hundred and forty (240) UZ bars were sintered (8 × 2 × 1 mm) and treated according to the factors (n = 15): Type of finishing/polishing procedure (Control - Ctrl; Ultra-fine Diamond Burr - FG; Medium grit diamond burr- MG; Stone Bur - Stone; Rubber - Rub; FG + Rub; MG + Rub; Stone + Rub), and “Glaze” (Without and With - Gl). The bars were hydrothermally degraded (24 h, 127 °C, 1.7 bar), submitted to roughness analysis and 3-point mini flexural strength (FS) test. Scanning Electron Microscopy (SEM), X-ray Diffraction (XDR), and Weibull analysis were performed. Data were analyzed by 2-way ANOVA and Tukey test (5%). Results: Finishing/Polishing’ and its interaction with ‘Glaze’ were statistically significant (P < 0.0001) for FS, unlike ‘Glaze’ alone (P = 0.8827). Rub (602.11 MPaA), Stone + Rub (555.50 MPaAB), and Ctrl (621.72 MPaA) showed superior FS, while FG_GL showed the lowest FS. Stone + Rub showed the highest Weibull modulus (13.15a). Ctrl_Gl (0.18 ± 0.02F μm) and Ctrl + Rub_Gl (0.29 ± 0.07F μm) showed the lowest roughness. Glaze (0.48B) reduced the roughness of the groups that did not receive it (1.56A), with MG (2.60 ± 0.69A μm) and FG (2.50 ± 0.7A μm) exhibiting rougher surfaces. Conclusions: Rubber polishers are ideal for minor adjustments to UZ while Stone followed by rubber is effective for greater abrasion without compromising mechanical strength. The application of glaze did not reduce mechanical strength and resulted in lower surface roughness compared to the non-glazed groups, with the exception of the FG groups.

Original languageEnglish
Article number106924
Pages (from-to)1-11
Number of pages11
JournalJournal of the Mechanical Behavior of Biomedical Materials
Volume164
Early online date3 Feb 2025
DOIs
Publication statusE-pub ahead of print - 3 Feb 2025

Bibliographical note

Publisher Copyright:
© 2025 Elsevier Ltd

Funding

This study was funded in part by the Coordination for the Development of Higher Education Personnel - Brazil (CAPES) - Grant Code 001 and National Council for Scientific and Technological Development (CNPq).

FundersFunder number
Coordination for the Development of Higher Education Personnel
Conselho Nacional de Desenvolvimento Científico e Tecnológico
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior001

    Keywords

    • Ceramics
    • Dental materials
    • Flexural strength
    • Zirconia

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