On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples.

U.A.T. Brinkman; F.D. Rinkema; A.J.H. Louter; T. Hankemeier

doi:10.1007/BF02272157

On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples.

U.A.T. Brinkman, F.D. Rinkema, A.J.H. Louter, T. Hankemeier

BioAnalytical Chemistry

Research output: Contribution to Journal › Article › Academic › peer-review

Abstract

An on-line, solid-phase extraction gas chromatography atomic-emission detection (SPE-GC-AED) system has been set up using an on-column interface to transfer 100 μl of desorbing solvent to the GC part of the system. Analytical characteristics such as recovery, precision and linearity of calibration plots were comparable with those of the off-line combination of SPE-GC-AED using organophosphorus pesticides as test compounds. The fully on-line set-up causes a marked improvement in detection because of the quantitative transfer of the analytes from the SPE module to the GC: detection limits are as low as 5-20 ng l

Original language	English
Pages (from-to)	119
Journal	Chromatographia
Volume	40
DOIs	https://doi.org/10.1007/BF02272157
Publication status	Published - 1995

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

Access to Document

10.1007/BF02272157

Persistent URL (handle)

Persistent link

Cite this

@article{bc023bd272bc433088c3c80f05ef8236,

title = "On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples.",

abstract = "An on-line, solid-phase extraction gas chromatography atomic-emission detection (SPE-GC-AED) system has been set up using an on-column interface to transfer 100 μl of desorbing solvent to the GC part of the system. Analytical characteristics such as recovery, precision and linearity of calibration plots were comparable with those of the off-line combination of SPE-GC-AED using organophosphorus pesticides as test compounds. The fully on-line set-up causes a marked improvement in detection because of the quantitative transfer of the analytes from the SPE module to the GC: detection limits are as low as 5-20 ng l",

author = "U.A.T. Brinkman and F.D. Rinkema and A.J.H. Louter and T. Hankemeier",

year = "1995",

doi = "10.1007/BF02272157",

language = "English",

volume = "40",

pages = "119",

journal = "Chromatographia",

issn = "0009-5893",

publisher = "Springer",

}

TY - JOUR

T1 - On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples.

AU - Brinkman, U.A.T.

AU - Rinkema, F.D.

AU - Louter, A.J.H.

AU - Hankemeier, T.

PY - 1995

Y1 - 1995

N2 - An on-line, solid-phase extraction gas chromatography atomic-emission detection (SPE-GC-AED) system has been set up using an on-column interface to transfer 100 μl of desorbing solvent to the GC part of the system. Analytical characteristics such as recovery, precision and linearity of calibration plots were comparable with those of the off-line combination of SPE-GC-AED using organophosphorus pesticides as test compounds. The fully on-line set-up causes a marked improvement in detection because of the quantitative transfer of the analytes from the SPE module to the GC: detection limits are as low as 5-20 ng l

AB - An on-line, solid-phase extraction gas chromatography atomic-emission detection (SPE-GC-AED) system has been set up using an on-column interface to transfer 100 μl of desorbing solvent to the GC part of the system. Analytical characteristics such as recovery, precision and linearity of calibration plots were comparable with those of the off-line combination of SPE-GC-AED using organophosphorus pesticides as test compounds. The fully on-line set-up causes a marked improvement in detection because of the quantitative transfer of the analytes from the SPE module to the GC: detection limits are as low as 5-20 ng l

U2 - 10.1007/BF02272157

DO - 10.1007/BF02272157

M3 - Article

SN - 0009-5893

VL - 40

SP - 119

JO - Chromatographia

JF - Chromatographia

ER -

On-line coupling of solid-phase extraction and gas chromatography with atomic emission detection for analysis of trace pollutants in aqueous samples.

Abstract

UN SDGs

Access to Document

Persistent URL (handle)

Fingerprint

Cite this